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The present invention relates to a dentifrice composition comprising a zeolite containing the basic ingredients described and to methods for producing the same.
2. Description of the Prior Art
Zeolite is a crystalline aluminosilicate having intergrowths of silica and alumina tetrahedra, and consists of a three-dimensional network having cavities and apertures. High-purity zeolite for use in dentifrice is generally obtained by crystallization of an aqueous reaction mixture, followed by drying, calcining, grinding and re-crystallization to reduce the water content. See, for example, Japanese Patent Application Laid-open No. 160720/1996.
A conventional method for producing high-purity zeolite (hereinafter referred to as «zeolite») is shown in FIG. 9. In the conventional method, a reaction mixture having a pH of at least about 8 is produced and ground to an average particle size of from about 0.1 to about 2 mm. The ground mixture is mixed with a sodium hydroxide solution, and is then agitated. The mixture is then left standing for a period of from about 1 to about 24 hours to crystallize zeolite. After the crystallization is completed, the resulting zeolite particles are separated, dried and then heated to a temperature of from about 180.degree. to about 290.degree. C. to calcine the zeolite. In the process of calcination, the dried zeolite particles are mixed with a sodium hydroxide solution to adjust the pH of the resultant mixture to 10-12, and then heated to a temperature of from about 200.degree. to about 450.degree. C. The calcined zeolite is separated from the mixture, and then ground and mixed with an aqueous hydrogen peroxide solution to obtain a dentifrice.
With the conventional method, however, the sodium hydroxide solution is used in the production of the reaction mixture, and is, therefore, of a lower quality in terms of
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